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有色金属(冶炼部分):2023,(7):68-74
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影响烧结钽坯料致密度的因素研究
解永旭
(宁夏东方钽业股份有限公司 宁夏石嘴山市 09522098738)
Factors Affecting Density of Sintered Tantalum Billet
XIE Yong-xu
(Ningxia Oriental Tantalun Intustry Co.)
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投稿时间:2023-03-18     修订日期:2023-04-06     录用日期:2023-04-07     网络发布日期:2023-06-16
中文摘要: 采用金属钽粉为原料,通过冷等静压成型、真空垂熔烧结、轧制、拉拔等粉末冶金加工工艺来制取电容器级钽丝。金属钽粉的微观形貌、粒度分布及化学成分等粉末特性,以及钽坯料加工过程及成型与烧结工艺过程特性,直接影响烧结后钽坯料的致密度,也将直接影响电容器级钽丝的理化性能。研究表明:钽粉的平均粒径在5.5~6.5 μm时有利于钽坯料的烧结;钽粉的化学杂质含量高、等静压压力小、烧结炉的气氛差等因素不利于钽坯料的致密。
中文关键词: 钽粉  钽坯料  粉末性能  垂熔烧结  密度
Abstract:Using metal tantalum powder as raw material, capacitor grade tantalum wire was prepared by powder metallurgy processes such as cold isostatic pressing, vacuum vertical melting sintering, rolling and drawing. The characteristics of tantalum metal powder, such as microstructure, particle size distribution and chemical composition, as well as the characteristics of tantalum blank processing, forming and sintering process, directly affect the density of tantalum blank after sintering, and also directly affect the physical and chemical properties of capacitor grade tantalum wire. The results show that when the average particle size of tantalum powder is 5.5—6.5 μm, it is beneficial to the sintering of tantalum blank. High chemical impurity content of tantalum powder, low isostatic pressure, poor sintering furnace atmosphere and other factors are not conducive to the density of tantalum blank.
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基金项目:国家自然科学基金创新群体资助项目(2021AAC01002)
引用文本:
解永旭.影响烧结钽坯料致密度的因素研究[J].有色金属(冶炼部分),2023(7):68-74.
XIE Yong-xu.Factors Affecting Density of Sintered Tantalum Billet[J].Nonferrous Metals (Extractive Metallurgy),2023(7):68-74.

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