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投稿时间:2022-05-27 修订日期:2022-05-27 录用日期:2022-05-27 网络发布日期:2022-06-17
投稿时间:2022-05-27 修订日期:2022-05-27 录用日期:2022-05-27 网络发布日期:2022-06-17
中文摘要: 研究钛元素对CBS系微晶玻璃的晶相、微观结构和介电性能的影响。结果表明,优选试验条件为,钛掺杂含量为2%、烧结制度为以3 ℃/min的速率升温到玻璃软化温度(701.0 ℃),保温1小时,以相同速率升温到高于析晶温度20 ℃的温度(881.9 ℃)下,保温2小时后随炉冷却。通过上述试验方案获得的样品,主晶相为硅灰石,微观结构上晶粒饱满且紧密相连,空隙较少,平均粒径3~5 μm,样品的介电常数分别为1.4(1 MHz)、1.3(10 MHz),介电损耗分别为3.9×10-3(1 MHz)、3.8×10-3(10 MHz)。
Abstract:Effects of titanium element doping on crystal phase, microstructure and dielectric properties of CBS glass ceramics were investigated. The results show the optimal test conditions include: titanium doping content is 2%, the sintering system is heated to glass softening temperature (701.0 ℃) with a rate of 3 ℃/min and held for 1 h, and then heated to a temperature (881.9 ℃) which is 20 ℃ above the crystallization temperature at the same rate. Finally, it is cooled with the furnace after holding at 881.9 ℃ for 2 h. The main crystalline phase of samples obtained by the above experimental scheme is wollastonite, and the grains are full and closely connected in microstructure, with less voids and an average particle size of 3—5 μm. The dielectric constant of the sample is 1.4 (1 MHz) and 1.3 (10MHz) respectively, and the dielectric loss is 3.9×10-3 (1 MHz) and 3.8×10-3 (10 MHz) respectively.
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基金项目:矿冶科技集团有限公司青年基金(04-2014-1)
引用文本:
袁朝新,高崇,王岩,黄海辉,王为振,靳冉公.钛掺杂对CBS微晶玻璃晶相、微观结构及介电性能的影响[J].有色金属(冶炼部分),2022(7):95-101.
YUAN Chao-xin,GAO Chong,WANG Yan,HUANG Hai-hui,WANG Wei-zhen,JIN Ran-gong.Effect of Ti-doping on Crystalline Phase, Microstructure and Dielectric Properties of CBS Glass Ceramics[J].Nonferrous Metals (Extractive Metallurgy),2022(7):95-101.
袁朝新,高崇,王岩,黄海辉,王为振,靳冉公.钛掺杂对CBS微晶玻璃晶相、微观结构及介电性能的影响[J].有色金属(冶炼部分),2022(7):95-101.
YUAN Chao-xin,GAO Chong,WANG Yan,HUANG Hai-hui,WANG Wei-zhen,JIN Ran-gong.Effect of Ti-doping on Crystalline Phase, Microstructure and Dielectric Properties of CBS Glass Ceramics[J].Nonferrous Metals (Extractive Metallurgy),2022(7):95-101.

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