本文已被:浏览 2039次 下载 2088次
投稿时间:2021-09-08 修订日期:2021-09-17 录用日期:2021-09-18 网络发布日期:2021-12-17
投稿时间:2021-09-08 修订日期:2021-09-17 录用日期:2021-09-18 网络发布日期:2021-12-17
中文摘要: 以陕西某地硅质钒矿为研究对象,进行了单一硫酸浸出、硫酸助浸、空白焙烧—浸出、硫酸熟化—常温水浸提钒探索试验,确定出硫酸熟化—常温水浸工艺更适用于硅质钒矿,同时考察了熟化温度、熟化时间、熟化硫酸及水用量、矿石粒度、浸出温度对钒浸出率的影响。结果表明,在熟化硫酸用量15%、熟化水用量10%、熟化温度130℃、熟化时间4 h、原矿粒度-8mm、熟料浸出液固比1.5、常温浸出3 h的条件下,可获得78%左右的钒浸出率。该硅质钒矿经硫酸熟化后水浸,浸出温度对钒浸出率影响小,可采用“熟化-柱浸(堆浸)”工艺进行提钒。
Abstract:Taking a siliceous vanadium ore in Shaanxi province as research object, exploration experiments of single sulfuric acid leaching, sulfuric acid assisted leaching, blank roasting-leaching, sulfuric acid slaking-normal temperature water leaching vanadium extraction process were carried out. It was determined that sulfuric acid slaking-normal temperature water leaching process was more suitable for siliceous vanadium ore. Effects of curing temperature, curing time, curing sulfuric acid and water dosage, ore particle size, and leaching temperature on vanadium leaching rate were investigated. The results show that leaching rate of vanadium is about 78% under the conditions including curing sulfuric acid dosage of 15%, curing water dosage of 10%, curing temperature of 130 ℃, curing time of 4 h, raw ore particle size of -8 mm, clinker leaching liquid to solid ratio of 1.5, and leaching time at room temperature of 3 h. Leaching temperature has little effect on vanadium leaching rate. The process of "curing - column leaching (heap leaching)" can be used to extract vanadium from this siliceous vanadium ore.
keywords: siliceous vanadium ore sulfuric acid curing vanadium extraction normal temperature water leaching
文章编号: 中图分类号: 文献标志码:
基金项目:陕西省创新人才推进计划资助项目(2020KJXX-053)
| 作者 | 单位 | |
| 曹欢* | 西安西北有色地质研究院有限公司 | 1443479028@qq.com |
| 吴天骄 | 西安西北有色地质研究院有限公司 | |
| 程倩 | 西安西北有色地质研究院有限公司 | |
| 宁新霞 | 西安西北有色地质研究院有限公司 | |
| 赵笑益 | 西安西北有色地质研究院有限公司 |
| Author Name | Affiliation | |
| CAO Huan | Xi ''an Northwest Nonferrous Geological Research Institute Co,LTD,Sh aanxi,Xi ''an | 1443479028@qq.com |
| WU Tian-jiao | ||
| CHEN Qian | ||
| NING Xin-xia | ||
| ZHAO Xiao-yi |
引用文本:
曹欢,吴天骄,程倩,宁新霞,赵笑益.硅质钒矿硫酸熟化常温水浸提钒[J].有色金属(冶炼部分),2022(1):67-72.
CAO Huan,WU Tian-jiao,CHEN Qian,NING Xin-xia,ZHAO Xiao-yi.Extracting Vanadium from Siliceous Vanadium Ore by Sulphuric Acid Curing and Water Leaching at Normal Temperature[J].Nonferrous Metals (Extractive Metallurgy),2022(1):67-72.
曹欢,吴天骄,程倩,宁新霞,赵笑益.硅质钒矿硫酸熟化常温水浸提钒[J].有色金属(冶炼部分),2022(1):67-72.
CAO Huan,WU Tian-jiao,CHEN Qian,NING Xin-xia,ZHAO Xiao-yi.Extracting Vanadium from Siliceous Vanadium Ore by Sulphuric Acid Curing and Water Leaching at Normal Temperature[J].Nonferrous Metals (Extractive Metallurgy),2022(1):67-72.

关注微信公众号