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有色金属(冶炼部分):2020,(1):52-55
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响应面法优化从电解锰阳极液中回收硒工艺
陈俊妃, 辛宇, 黄丽燕, 覃兆财, 粟海锋
(广西大学化学化工学院)
Response Surface Optimization of Process Parameters for Recovery of Selenium from Electrolytic Manganese Anolyte
CHEN Junfei, XIN Yu, HUANG Liyan, QIN Zhaocai, SU Haifeng
(School of Chemistry and Chemical Engineering,Guangxi University)
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投稿时间:2019-08-17     修订日期:2019-08-21     录用日期:2019-08-23     网络发布日期:2019-12-18
中文摘要: 采用响应面设计优化铁炭微电解法回收电解锰阳极液中硒的工艺条件,研究搅拌速率、铁炭比和反应时间对硒回收率的影响。结果表明,各因素对硒回收率的影响大小顺序为:搅拌速率>铁炭比>反应时间,三者之间两两的交互作用均较弱。最优工艺条件为:搅拌速率199 r/min、铁炭比1.94 g/g、反应时间192 min。在此条件下,硒的回收率可达到96.34%,与模型预测值96.52 %无显著差异。
Abstract:Response surface methodology was applied to optimize extracting process parameters to recover selenium from electrolytic manganese anolyte by iron-carbon micro-electrolysis technology. Stirring speed, reaction time, and ratio of iron/carbon were selected as three independent variables on selenium extraction rate as response. The results show that effect sequence of factors on selenium extraction rate is stirring rate, iron/carbon ratio, and reaction time. Interaction between two of three factors was weak. The optimum extracting process parameters include stirring speed of 199 r/min, reaction time of 192 min, and ratio of iron/carbon of 1.94 g/g. Under these conditions, selenium extraction rate is 96.34%, which is not significantly different from value of 96.52% predicted by the model.
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基金项目:国家自然科学基金资助项目(51664002);广西自然科学基金重点项目(2018GXNSFDA281018)
引用文本:
陈俊妃,辛宇,黄丽燕,覃兆财,粟海锋.响应面法优化从电解锰阳极液中回收硒工艺[J].有色金属(冶炼部分),2020(1):52-55.
CHEN Junfei,XIN Yu,HUANG Liyan,QIN Zhaocai,SU Haifeng.Response Surface Optimization of Process Parameters for Recovery of Selenium from Electrolytic Manganese Anolyte[J].Nonferrous Metals (Extractive Metallurgy),2020(1):52-55.

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