Abstract:Traditional process to produce palladium dichloride has the disadvantages of high purity requirement of raw materials, long production cycle, high loss rate of palladium and difficulty to control reaction end point. One innovation process to produce palladium dichloride applying diamminedichloropalladium as raw material under relative gentle reaction conditions was put forward. Palladium content of in product is as high as 59.72%. Its composition and microstructures are analyzed and characterized by chemical analysis, XRD and SEM.